Kosata Bedrich       Example 40    <<       >>       BOOK      KEYWORDS      EXAMPLES      HELP     

You treated naphtalene-1,6-diol with acetyl chloride, and you obtained two products. One of them was a product of acetylation in position 2. The second product is crystalic, with mp=106-107. What is it?
 
     Query 1         Query 2   

     Query 1       HOME      Hitset 1     

This question is rather difficult. Firstly we try to find these reactions of naphtalene-1,6-diol where reagent is acetylchloride.

  Q1    54 hits  

  Note:  
the reactions of diol
  Q2    2839 hits  
       (rx.rgt = accl or rx.rgt = "acetyl chloride")       
  Note:  
then acetyl chloride as the reagent
  Q3    0 hits  
       .Q1 or .Q2       
  Note:  
finally, we put them together. Whooops, nothing found
     Hitset 1       HOME      Query 1     

  Comments:

     Query 2       HOME      Hitset 2     

We can try reactions of diol that leads to product with mp=100-110 (we can't be sure of exact mp=106-107)

  Q1    54 hits  

  Note:  
diol first
  Q2    258838 hits  
       mp = 100-110       
  Note:  
all compounds with desired melting point
  Q3    4 hits  
       .Q1 and .Q2       
  Note:  
put them both together
     Hitset 2       HOME      Query 2     
 1 

387787
 2 

2276905
  3 

7762777

  Comments:
 3. and this is the one we searched for  

 

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